DCSSI - UNIVERSITA' DEGLI STUDI DI MILANO - sito del Prof.Gianfranco Ciani -

       

            

 

ELENCO DELLE PUBBLICAZIONI DEL PROF. GIANFRANCO CIANI

( parte 1 di 3 )

Elenco comunicazioni a congressi

 

1)

A monocapped octahedral form of Rh7 (metal atom) cluster in the tetramethylammonium salt of hexadecacarbonylheptarhodate trianion.
V. G. Albano, P. L. Bellon e G. Ciani.
J. C. S. Chem. Commun., (1969) 1024.

2)

A tetrakis-(m3-hydroxometal) group in the crystal structure of the triphenylphosphine oxide adduct of [Mo(OH)(CO)2(NO)]4.
V. G. Albano, P. L. Bellon, G. Ciani e M. Manassero.
J. C. S. Chem. Commun., (1969) 1242.

3)

Structure of the tri-(m-hydroxo)hexacarbonylditungstate(0) trianion in the salt K3[W2(OH)3(CO)6].2H2O.
V. G. Albano, G. Ciani e M. Manassero.
J. Organomet. Chem., 25 (1970) C55.

4)

Molybdenum and tungsten hydroxocarbonylhydrides and hydroxocarbonylnitrosyls.
U. Sartorelli, L. Garlaschelli, G. Ciani e G. Bonora.
Inorg. Chim. Acta, 5 (1971) 191.

5)

Absorption correction in the Weissenberg and precession geometries.
G. Ciani, M. Manassero e M. Sansoni.
J. Appl. Crystallogr., 4 (1971) 173.

6)

Crystal and molecular structure of (dithioformato)bis(triphenylphosphine)dicarbonylrhenium, Re(HCS2)(CO)2[P(C6H5)3]2.
V. G. Albano, P. L. Bellon e G. Ciani.
J. Organomet. Chem., 31 (1971) 75.

7)

The crystal and molecular structure of the diphenylethylphosphine oxide adduct of
tetrakis-(
m3-hydroxotricarbonylhydridotungsten), [W(OH)(CO)3H]4.4OPPh2Et.
V. G. Albano, G. Ciani, M. Manassero e M. Sansoni.
J. Organomet. Chem., 34 (1972) 353.

8)

Crystal and molecular structure of monoclinic di-m-chloro-tris(triphenylphosphine)dicopper(I), Cu2Cl2(PPh3)3.
V. G. Albano, P. L. Bellon, G. Ciani e M. Manassero.
J. C. S. Dalton Trans., (1972) 171.

9)

A square-pyramidal Mn(II) species in the crystal structure of iodotetrakis(triphenylphosphineoxide)manganese(II) diiodotetracarbonylmanganate(I), [MnI(OPPh3)4][MnI2(CO)4].
G. Ciani, M. Manassero e M. Sansoni.
J. Inorg. Nucl. Chem., 34 (1972) 1760.

10)

Stereochemistry of tetrahedral complexes of group VIII metals. Crystal and molecular structures of Co(CO)2(NO)(PPh3) and Co(CO)(NO)(PPh3)2.
V. G. Albano, P. L. Bellon e G. Ciani.
J. Organomet. Chem., 38 (1972) 155.

11)

A novel mixed platinum-iron cluster compound: structure of triangulo-tetracarbonyliron-carbonyltris(triphenylphosphite)diplatinum.
V. G. Albano, G. Ciani, M. I. Bruce, G. Show e F. G. A. Stone.
J. Organomet. Chem., 42 (1972) C99.

12)

Crystal and molecular structure of dichlorotris-[1,2-bis(diphenylphosphino)ethane]dicopper(I)-bisacetone.
V. G. Albano, P. L. Bellon e G. Ciani.
J. C. S. Dalton Trans., (1972) 1938.

13)

Preparation and X-ray crystal structure of tetranitrosylbis(triphenylphosphine)di-iridium.
M. Angoletta, G. Ciani, M. Manassero e M. Sansoni.
J. C. S. Chem. Commun., (1973) 789.

14)

The crystal and molecular structure of tricyclic tetracarbonylironcarbonyltris(triphenylphosphite)diplatinum.
V. G. Albano e G. Ciani.
J. Organomet. Chem., 66 (1974) 311.

15)

Stereochemistry of tetrahedral complexes of group VIII metals. Crystal and molecular structures of dinitrosylcarbonyltriphenylphosphineiron, Fe(NO)2(CO)(PPh3), and of dinitrosylbis(triphenylphosphine)iron, Fe(NO)2(PPh3)2.
V. G. Albano, A. Araneo, P. L. Bellon, G. Ciani and M. Manassero.
J. Organomet. Chem., 67 (1974) 413.

16)

Crystal and molecular structure of the bis(tetramethylammonium) octa-m3-carbonyl-hexacarbonyl-octahedro-dinickeltetracobaltate(2-).
V. G. Albano, G. Ciani e P. Chini.
J. C. S. Dalton Trans., (1974) 432.

17)

The twinned and disordered crystal structure of tetrahedral tri-m-carbonylenneacarbonyldicobaltdiiridium.
V. G. Albano, G. Ciani e S. Martinengo.
J. Organomet. Chem., 78 (1974) 265.

18)

Synthesis and characterization of [Rh7(CO)16X]2- anions (X = Br, I).
S. Martinengo, P. Chini, G. Giordano, A. Ceriotti, V. G. Albano e G. Ciani.
J. Organomet. Chem., 88 (1975) 375.

19)

The crystal and molecular structure of the new cluster dianion m-iodotetra-m3-carbonyl-di-m-carbonyldecacarbonyl-polyhedro-heptarhodate(2-) in its tetraethylammonium salt.
V. G. Albano, G. Ciani, S. Martinengo, P. Chini e G. Giordano.
J. Organomet. Chem., 88 (1975) 381.

20)

A new carbonylhydridorhenium cluster.
V. G. Albano, G. Ciani, M. Freni e P. Romiti.
J. Organomet. Chem., 96 (1975) 259.

21)

Reactions of the pentahalogenonitrosylrhenate anions [Re(NO)X5]2- (X = Cl, Br) with solvents.
G. Ciani, D. Giusto, M. Manassero e M. Sansoni.
Inorg. Chim. Acta, 14 (1975) L25.

22)

Nitrosyl complexes of rhenium. Crystal and molecular structure of the tetraethylammonium salts of tetrabromo(ethanol)nitrosylrhenate(II) and of acetonitriletetrabromonitrosylrhenate(II).
G. Ciani, D. Giusto, M. Manassero e M. Sansoni.
J. C. S. Dalton Trans., (1975) 2156.

23)

Hexagonal close packing of metal atoms in the new polynuclear anions [Rh13(CO)24H5-n]n- (n = 2 or 3);
X-ray structure of [(Ph
3P)2N]2[Rh13(CO)24H3].
V. G. Albano, A. Ceriotti, P. Chini, G. Ciani, S. Martinengo e W. M. Anker.
J. C. S. Chem. Commun., (1975) 859.

24)

Synthesis and reactions of dihydridonitrosyltris(triphenylphosphine)rhenium.
D. Giusto, G. Ciani e M. Manassero.
J. Organomet. Chem., 105 (1976) 91.

25)

Nitrosyl complexes of rhenium. Part 2. Crystal and molecular structure of dihydridonitrosyltris(triphenylphosphine)rhenium(I)-benzene(2/1).
G. Ciani, D. Giusto, M. Manassero e A. Albinati.
J. C. S. Dalton Trans., (1976) 1943.

26)

Synthesis and X-ray characterization of the dianions trihydridodecacarbonyltrirhenate (2-) and
trihydrido-
m3-oxoenneacarbonyltrirhenate (2-).
A. Bertolucci, M. Freni, P. Romiti, G. Ciani, A. Sironi e V.G. Albano.
J. Organomet. Chem., 113 (1976) C61.

27)

Synthesis and characterization of the tetranuclear anions [Rh4(CO)11(COOCH3)]- and [Rh4(CO)11]2-.
S. Martinengo, A. Fumagalli, P. Chini, V. G. Albano e G. Ciani.
J. Organomet. Chem., 116 (1976) 333.

28)

The crystal and molecular structure of hepta-m-carbonyltetracarbonyl-tetrahedro-tetrarhodate(2-) in its bis(triphenylphosphine)iminium salt.
V. G. Albano, G. Ciani, A. Fumagalli, S. Martinengo e W. M. Anker.
J. Organomet. Chem., 116 (1976) 343.

29)

A novel tetrahedral hydridocarbonylrhenium cluster: preparation and X-ray structure of [H4Re4(CO)13]2-.
A. Bertolucci, G. Ciani, M. Freni, P. Romiti, V.G. Albano e A. Albinati.
J. Organomet. Chem., 117 (1976) C37.

30)

Characterization of a copper(II) complex formed by reaction of acrylonitrile with N-Salicylideneglycinatocopper(II).
L. Casella, M. Gullotti, A. Pasini, M. Manassero, M. Sansoni, G. Ciani e A. Sironi.
Inorg. Chim. Acta, 20 (1976) L31.

31)

Stabilization of carbonyl clusters by a carbide atom. Synthesis and characterization of [Co8(CO)18C]2- and of paramagnetic [Co6(CO)14C]- anions.
V. G. Albano, P. Chini, G. Ciani, M. Sansoni, D. Strumolo, B. T. Heaton e S. Martinengo.
J. Amer. Chem. Soc., 98 (1976) 5027.

32)

The crystal and molecular structure of the tetraethylammonium salt of tetrahydridopentadecacarbonyltetrarhenate(2-) in two crystallographic forms.
G. Ciani, V. G. Albano e A. Immirzi.
J. Organomet. Chem., 121 (1976) 237.

33)

Synthesis and X-ray characterization of Rh4(CO)8[P(OPh)3]4 and Rh6(CO)12[P(OPh)3]4.
G. Ciani, L. Garlaschelli, M. Manassero, U. Sartorelli e V. G. Albano.
J. Organomet. Chem., 129 (1977) C25.

34)

Products of the reaction of Re2(CO)10 with methanolic KOH. The crystal and molecular structure of the trimethylbezylammonium salt of hexa-m2-hydridododecacarbonyl-tetrahedro-tetrarhenate (2-).
G. Ciani, A. Sironi e V.G. Albano.
J. Organomet. Chem., 136 (1977) 339.

35)

Synthesis and X-ray structure of the anion tetra-m-hydridodecacarbonyl-triangulo-trirhenate (1-).
G. D'Alfonso, M. Freni, P. Romiti, G. Ciani, A. Sironi e A. Albinati.
J. Organomet. Chem., 136 (1977) C49.

36)

Crystal and molecular structure of Bis(tetraethylammonium)
1,2;2,3;3,1-Tri-
m-hydrido-m3-oxo-1,1,1,2,2,2,3,3,3,-enneacarbonyl-triangulo-trirhenate(2-).
G. Ciani, A. Sironi e V.G. Albano.
J. C. S. Dalton Trans., (1977) 1667.

37)

Reactions of pentachloro- and pentabromonitrosylrhenate(II) anions with N-donor ligands.
G. Ciani, D. Giusto, M. Manassero e M. Sansoni.
Gazz. Chim. Ital., 107 (1977) 429.

38)

Stereoselective effects in the coordination of amino acids. Crystal structure of the copper(II) complex with the Schiff base between (1R)-3-hydroxymethylenecamphor and (S)-phenylalanine.
L. Casella, M. Gullotti, A. Pasini, G. Ciani, M. Manassero e A. Sironi.
Inorg. Chim. Acta, 26 (1978) L1.

39)

New carbide clusters in the cobalt sub-group. Part 5. Crystallographic characterization of deca-m-carbonyl-carbido-octacarbonyl-polyhedro-octacobaltate(2-) in its bis(benzyltrimethylammonium) salt.
V.G. Albano, P. Chini, G. Ciani, S. Martinengo e M. Sansoni.
J. C. S. Dalton Trans., (1978) 468.

40)

A new tetrahedral cluster of iridium containing two terminal hydrides. Synthesis and X-ray structure of dihydridodecacarbonyl-tetrahedro-tetrairidate(2-).
G. Ciani, M. Manassero, V. G. Albano, F. Canziani, G. Giordano, S. Martinengo e P. Chini.
J. Organomet. Chem., 150 (1978) C17.

41)

New tetrahedral cluster compounds of iridium. Synthesis of the anions [Ir4(CO)11X]- (X = Cl, Br, I, CN, SCN) and X-ray structure of [PPh4][Ir4(CO)11Br].
P. Chini, G. Ciani, L. Garlaschelli, M. Manassero, S. Martinengo, A. Sironi e F. Canziani.
J. Organomet. Chem., 152 (1978) C35.

42)

Isolation, reactions and X-ray structure of tetraethylammonium dihydrido tetracarbonylrhenate.
G. Ciani, G. D'Alfonso, M. Freni, P. Romiti e A. Sironi.
J.Organomet. Chem., 152 (1978) 85.

43)

Nitrosyl complexes of rhenium. Part 3. Crystal and molecular structure of tetraethylammonium tetrachloronitrosyl(pyridine)rhenate(1-).
G. Ciani, D. Giusto, M. Manassero e M. Sansoni.
J. C. S. Dalton Trans., (1978) 798.

44)

Pyrolyses of the anion dihydridotetracarbonylrenhate. Crystal and molecular structure of bis(tetraethylammonium)m-hydrido-dodecacarbonyl-triangulo-trirhenate(2-).
G. Ciani, G. D'Alfonso, M. Freni, P. Romiti e A. Sironi.
J. Organomet. Chem., 157 (1978) 199.

45)

Analogues of metallic lattices in rhodium carbonyl cluster chemistry. Synthesis and X-ray structure of the [Rh15(m-CO)14(CO)13]3- and [Rh14(m-CO)16(CO)9]4- anions showing a stepwise hexagonal close-packed / body-centered cubic interconversion.
S. Martinengo, G. Ciani, A. Sironi e P. Chini.
J. Amer. Chem. Soc., 100 (1978) 7096.

46)

Synthesis and characterization of the anion-tetra-m-hydridoiodo pentadecacarbonyl tetrarhenate(1-).
G. Ciani, G. D'Alfonso, M. Freni, P. Romiti e A. Sironi.
J. Organomet. Chem., 170 (1979) C15.

47)

Structural characterization of the tri(m-alkoxy)hexacarbonyldirhenate(I) anion.
G. Ciani, A. Sironi e A. Albinati.
Gazz. Chim. Ital., 109 (1979) 615.

48)

High nuclearity carbonyl cluster of rhodium. Part 1. Crystallographic characterization of dodeca-m-carbonyl-dodecacarbonyldihydrido-polyhedro-tridecarhodate(3-) in its benzyltriphenylphosphonium salt.
V.G. Albano, G. Ciani, S. Martinengo e A. Sironi.
J. C. S. Dalton Trans., (1979) 978.

49)

Synthesis and X-ray crystal structure of the anion [Co6(CO)14(m-CO)2P]-; an example of a semi-interstitial phosphide.
P. Chini, G. Ciani, S. Martinengo, A. Sironi, L. Longhetti e B. T. Heaton.
J. C. S. Chem. Commun., (1979) 188.

50)

Synthesis and X-ray crystal structure of the [Rh5(CO)8(m-CO)6I]2- anion containing a trigonal bipyramidal rhodium cluster.
S. Martinengo, G. Ciani e A. Sironi.
J. C. S. Chem. Commun., (1979) 1059.

51)

Synthesis and X-ray characterization of the [M6N(m-CO)9(CO)6]- (M = Co, Rh) anions. A new class of metal carbonyl cluster compounds containing an interstitial nitrogen atom.
S. Martinengo, G. Ciani, A. Sironi, B.T. Heaton e J. Mason
J. Amer. Chem. Soc., 101 (1979) 7095.

52)

Reactions of the unsaturated anions [H3Re3(CO)10]2- and [H4Re3(CO)10]- with iodine in various solventes.
X-ray characterization of the derivative H
3Re3(CO)10(Py)2.
G. Ciani, G. D'Alfonso, M.Freni, P. Romiti e A. Sironi.
J. Organomet. Chem., 186 (1980) 353.

53)

New carbide clusters in the cobalt sub-group. Part 6. Crystallographic characterization of the tetramethylammonium salt of the paramagnetic anion carbidohexa-m-carbonyl-octacarbonyl-polyhedro-hexacobaltate(1-).
V.G. Albano, P. Chini, G. Ciani, M. Sansoni e S. Martinengo.
J. C. S. Dalton Trans., (1980) 163.

54)

Synthesis and structural characterization of the anion [Rh6(CO)14(h3-C3H5)]-.
G. Ciani, A. Sironi, P. Chini, A. Ceriotti e S. Martinengo.
J. Organomet. Chem., 192 (1980) C39.

55)

A novel hydridic high-nuclearity rhodium cluster: synthesis and X-ray crystal structure of the anion
[Rh
14H(m-CO)15(CO)10]3-.
G. Ciani, A. Sironi e S. Martinengo.
J. Organomet. Chem., 192 (1980) C42.

56)

The stoichiometries of high nuclearity transition metal carbonyl cluster compounds. I. Compact close-packed clusters.
G. Ciani e A. Sironi.
J. Organomet. Chem., 197 (1980) 233.

57)

The crystal and molecular structure of the tetraphenylphosphonium salt of the anion
bromotri-
m-carbonyloctacarbonyl-tetrahedro-tetrairidate(-1).
G. Ciani, M. Manassero e A. Sironi.
J. Organomet. Chem., 199 (1980) 271.

58)

Synthesis and X-Ray structural characterization of the [Rh22(m3-CO)7(m-CO)18(CO)12]4- anion, containing a large close-packed cluster with an ABAC sequence of compact layers.
S. Martinengo, G. Ciani e A. Sironi.
J. Amer. Chem. Soc., 102 (1980) 7564.

59)

Synthesis and X-ray crystal structure of the novel high nuclearity rhodium-cluster dianion
[Rh
14(m-CO)15(CO)11]2-.
S. Martinengo, G. Ciani e A. Sironi.
J. C. S. Chem. Commun., (1980) 1140.

60)

Crystal and molecular structure of tetra-m3-carbonyl-octacarbonyltetrakis(triphenyl phosphite)-octahedro-hexarhodium.
G. Ciani, M. Manassero e V. G. Albano.
J. C. S. Dalton Trans., (1981) 515.

61)

High nuclearity carbonyl clusters of rhodium. Part 2. Crystal and molecular structure of the tetramethylammonium salt of dodeca-m-carbonyl-dodecacarbonylhydrido-polyhedro-tridecarhodate(4-)-1-methylpyrrolidin-2-one (1/3).
G. Ciani, A. Sironi e S. Martinengo.
J. C. S. Dalton Trans., (1981) 519.

62)

Dioxomolybdenum (VI) complexes of quadridentate chiral Schiff bases and the crystal and molecular structure of dioxo[(2R)-propane-1,2-diylbis[(salicylideneiminato)]molybdenum(VI).
M. Gullotti, A. Pasini, G. M. Zanderighi, G. Ciani e A. Sironi.
J. C. S. Dalton Trans., (1981) 902.

63)

Structural characterization of the anions [Rh6(CO)15X]- [X = COEt and CO(OMe)].
G. Ciani, A. Sironi, P. Chini e S. Martinengo.
J. Organomet. Chem., 213 (1981) C37.

64)

Carbide clusters in the cobalt sub-group. VIII. Crystallographic characterization of the anion dicarbido-undeca-m-carbonyl-undecacarbonyl-polyhedro-undecacobaltate(3-) as its tris(benzyltrimethylammonium) salt.
V.G. Albano, D. Braga, G. Ciani e S. Martinengo.
J. Organomet. Chem., 213 (1981) 293.

65)

Synthesis, crystal structure and absolute configuration of the menthyl-cyclopentadienyl complex of
ruthenium (+)
578-(h5-MCp)Ru(CO)P(C6H5)3Cl.
E. Cesarotti, G. Ciani e A. Sironi.
J. Organomet. Chem., 216 (1981) 87.

 

 

 

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